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In general, the headspace equilibrium temperature 1.5ml headspace crimp vials<the temperature of the loop <the temperature of the headspace transmission line is about ten degrees.
The equilibrium temperature is generally 80 ° C, of course, the boiling point of the compound is very high, the test substance can be set higher, the balance time can be set to 30 ~ 60min.
This is the end of the introduction of How to set up the headspace sampling device in gas chromatography? I hope it can help you.